A Chromatographic Method for Separating and Identifying Intact 4-Methylthio-3-Butenyl Glucosinolate in Japanese Radish (Raphanus sativus L.)
Japan Agricultural Research Quarterly
| ISSN | 00213551 |
|---|---|
| NII recode ID (NCID) | AA0068709X |
Full text
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To isolate and measure intact 4-methylthio-3-butenyl glucosinolate (4MTB-GSL) in Japanese radish, we applied a paired ion chromatography method that uses tetradecylammonium ions (TDA) as counter ions. 4MTB-GSL was isolated as ammonium salts from the root of a Japanese radish and identified on the basis of myrosinase treatment, aglycon detection, negative fast atom bombardment (FAB)-mass spectra, and a UV spectrum. The linearity of the prepared standard solution and recovery of that added to Japanese radish extracts were high.
| Date of issued | |
|---|---|
| Creator | ITO Hidekazu HORIE Hideki |
| Subject |
FAB-MS kaiware daikon paired ion sprout UV spectrum |
| Publisher | Japan International Research Center for Agricultural Sciences |
| Available Online | |
| NII resource type vocabulary | Journal Article |
| Volume | 42 |
| Issue | 2 |
| spage | 109 |
| epage | 114 |
| DOI | 10.6090/jarq.42.109 |
| Rights | Japan International Research Center for Agricultural Sciences |
| Language | eng |